In the past, I've always found the IUCr crystallographic pamphlets to be useful when teaching diffraction. They've reorganized their website to make their educational resources easier to find. On this link, you can find the IUCr teaching pamphlets, a short description of how to grow crystals, and other crystallography web resources.
Teaching Pamphlet Topics
http://assign3.chem.usyd.edu.au/spectroscopy/index.php
A series of Java tools for learning about the relationship between molecular parameters (size, mass etc) and the form of the spectral trace. These cover rotational, vibrational, ro-vibrational and electronic spectroscopy.
The University of Oklahoma has put together a nice website on Crystallography which includes a standard introduction to crystallography & crystal symmetry. I also like some of the features that you don't normally come across including evaluating crystal structures and twinning.
At the end of my inorganic course, I teach several "cool" analytical techniques that inorganic chemists use. These techniques are discussed within the context of bioinorganic chemistry, and I typically cover EXAFS/XANES, X-ray crystallography, EPR and Mössbauer. I provide this website to the students as supplemental reading material for X-ray crystallography, which is not typically covered in depth in an introductory inorganic text. The first link is the main website, but I usually only focus on the 2nd and 3rd links which covering the experimental setup for an X-ra
We have developed an online tutorial that demonstrates the fundamental principles and applications of the various types of spectroscopy that students will encounter in the inorganic chemistry laboratory, namely infrared spectroscopy (IR), nuclear magnetic resonance spectroscopy (NMR) and UV-visible spectroscopy (UV-vis). The tutorial has been designed as a stand-alone interactive resource that can either introduce the fundamental aspects of spectroscopy from first principles or serve as a supplement for students who prefer to learn visually in an individual setti
House (Inorganic chemistry): The book is divided into 5 parts: first, an introductory section on atomic structure, symmetry, and bonding; second, ionic bonding and solids; third, acids, bases and nonaqueous solvents; fourth, descriptive chemistry; and fifth, coordination chemistry. The first three sections are short, 2-4 chapters each, while the descriptive section (five chapters) and coordination chemistry section (seven chapters covering ligand field theory, spectroscopy, synthesis and reaction chemistry, organometallics, and bioinorganic chemistry.) are longer. Each chapter includes
Miessler and Tarr is an inorganic textbook which is is best suited to an upper-division one-semester inorganic course, though there is more material than can be covered in a single semester, so some choice of topics is necessary. It is very well suited for a course oriented around structure, bonding, and reaction chemistry of transition metal compounds, but is very limited in its treatment of solids, main-group, descriptive chemistry, and bioinorganic. Pchem would be helpful but is not necessary. In particular, the treatment of MO theory is very in-depth. The quality of end-of chapter p
Housecroft and Sharpe (Inorganic Chemistry, 3ed): This is a comprehensive inorganic textbook designed primarily for students at the Junior/Senior level. P-Chem would not be needed as a prerequisite for this text, but would be helpful. It includes both theoretical and descriptive material along with special topics, enough for a two semester course though it is easily adaptable to a one-semester "advanced inorganic" course by choosing only some topics. It is written in a clear and generally readable style and the full-color graphic contribute to student understanding.