Preparation and Spectroscopic Characterization of the Classical Coordination Compounds Copper(II) and Silver(II) Picolinate.
Description
Normal.dotm
0
0
1
199
1138
Kalamazoo College
9
2
1397
12.0
Powder Diffraction Crystallography Instructional Materials
Description
Brian Toby (Argonne National Labs) has assebled an excellent series of tutorials on using the Rietveld analysis technique for powder diffraction data. Tutorials range from an "Introduction to Crystallography" and "Getting Started with Rietveld" to using the "Le Bail Intensity Extraction" Method to "Advanced Rietveld Techniques."
Pyrophoric Liquid Safety Video
Description
This website is a video put out by UCLA and is a good general introduction to using pyrophorics. It would be good for required viewing for ALL researchers who intend to use Grignards, alkyl metals, organometallics, LiH, etc.
Updated June 2015 to provide a new link; the old link no longer worked.
Student-Led Organometallics
Description
I teach my organometallics course, a junior/senior level half-course, entirely as student-led presentations of the primary literature. In the past, the course was populated almost entirely with seniors who had already taken a one-semester advanced inorganic course. This past year, I taught it to juniors and seniors, and the juniors had not taken inorganic yet. A description of the course first appeared in J. Chem. Educ. in 2007 (link below). This VIPEr learning object is an update of the original paper based on my experience over the past two years.
Bioinorganic Techniques in a Nutshell
Description
This website is from the Center for Metalloenzyme Studies at the University of Georgia. It contains brief summaries of common techniques used in bioinorganic chemistry. I really liked that for each technique lists what kind of information you can obtain, as well as what the limitations of the method are. It also provides examples of what kinds of questions can be answered with each technique. It does not provide in-depth information about how each method works, but rather simply lists the basic facts about each technique.
Energy Nuggets: Engineering Viruses to Build a Better Battery
Description
This literature discussion activity is one of a series of “Energy Nuggets,” small curricular units designed to illustrate: The Role of Inorganic Chemistry in the Global Challenge for Clean Energy Production, Storage, and Use.
Energy Nuggets: Wise Energy Use – The Challenge of Nitrogen Fixation
Description
This literature discussion activity is one of a series of “Energy Nuggets,” small curricular units designed to illustrate: The Role of Inorganic Chemistry in the Global Challenge for Clean Energy Production, Storage, and Use.
Fourier Transforms and the Phase Problem
Description
At the end of my inorganic course, I teach several "cool" spectroscopic techniques that inorganic chemists use. These techniques are discussed within the context of bioinorganic chemistry, and I typically cover EXAFS/XANES, X-ray crystallography, EPR and Mössbauer.
This website introduces (or reviews) Fourier Transforms in a neat graphical way, but most importantly, illustrates the phase problem. Given the intensities from your crystal and the phases from your model, the phases are more important! Which is too bad, as we don't have ready access to that information.
Energy Nuggets: MOF’s for CO2 Sequestration
Description
This literature discussion activity is one of a series of “Energy Nuggets,” small curricular units designed to illustrate: The Role of Inorganic Chemistry in the Global Challenge for Clean Energy Production, Storage, and Use.
Introduction to X-ray crystallography
Description
At the end of my inorganic course, I teach several "cool" analytical techniques that inorganic chemists use. These techniques are discussed within the context of bioinorganic chemistry, and I typically cover EXAFS/XANES, X-ray crystallography, EPR and Mössbauer. I provide this website to the students as supplemental reading material for X-ray crystallography, which is not typically covered in depth in an introductory inorganic text. The first link is the main website, but I usually only focus on the 2nd and 3rd links which covering the experimental setup for an X-ra