[TaCl2(NMe2)3]2
We're trying to follow the old Chisholm prep from 1981 (http://dx.doi.org/10.1021%2Fic50220a049) and are getting super low yields. Any words of advice?
Ta(NMe2)5 + 2 TMSCl --> [TaCl2(NMe2)3]2 + 2 TMSNMe2
Forums
We're trying to follow the old Chisholm prep from 1981 (http://dx.doi.org/10.1021%2Fic50220a049) and are getting super low yields. Any words of advice?
Ta(NMe2)5 + 2 TMSCl --> [TaCl2(NMe2)3]2 + 2 TMSNMe2